VILLANI Claudio

Full Professor
Head of Department
Settore Scientifico-Disciplinare: 
CHIM/06
Informazioni personali
Curriculum vitae (it): 
Curriculum vitae (en): 
Didattica
Ricerca

Pubblicazioni scientifiche

Anno: 2021
Titolo pubblicazione Rivista Anno link Scopus link Sci_Dir
Chromatographic separation of the interconverting enantiomers of imidazo- and triazole-fused benzodiazepines Journal of Chromatography A 2021 Sci_Dir
Comparison of Coated and Immobilized Chiral Stationary Phases Based on Amylose tris-[(S)-α-Methylbenzylcarbamate] for the HPLC Enantiomer Separation of α-Lipoic Acid and Its Reduced Form Molecules (Basel, Switzerland) 2021 Sci_Dir
Molecular recognition of the hplc whelk-o1 selector towards the conformational enantiomers of nevirapine and oxcarbazepine International Journal of Molecular Sciences 2021 Sci_Dir
Multimilligram-scale production implementation of atropisomers of 2,2′-bis(2,2′-bithiophene-5-yl)-3,3′-bithianaphthene Chirality 2021 Sci_Dir
Salivary caffeine in Parkinson's disease. Scientific Reports 2021 Sci_Dir
Static vs. Dynamic electrostatic repulsion reversed phase liquid chromatography: Solutions for pharmaceutical and biopharmaceutical basic compounds Separations 2021 Sci_Dir
Anno: 2020
Titolo pubblicazione Rivista Anno link Scopus link Sci_Dir
Direct HPLC enantioseparation of chemopreventive chiral isothiocyanates sulforaphane and iberin on immobilized amylose-based chiral stationary phases under normal-phase, polar organic and aqueous conditions Talanta 2020 Sci_Dir
High–throughput enantioseparation of Nα–fluorenylmethoxycarbonyl proteinogenic amino acids through fast chiral chromatography on zwitterionic-teicoplanin stationary phases Journal of Chromatography A 2020 Sci_Dir
Single-run reversed-phase HPLC method for determining sertraline content, enantiomeric purity, and related substances in drug substance and finished product Journal of Pharmaceutical Analysis 2020 Sci_Dir
Synthesis, Resolution, Configurational Stability, and Properties of Cationic Functionalized [5]Helicenes Journal of Organic Chemistry 2020 Sci_Dir
Ultra-high performance separation of basic compounds on reversed-phase columns packed with fully/superficially porous silica and hybrid particles by using ultraviolet transparent hydrophobic cationic additives Journal of Separation Science 2020 Sci_Dir
Unusual complexation behavior between daclatasvir and γ-Cyclodextrin. A multiplatform study Journal of Chromatography A 2020 Sci_Dir
Anno: 2019
Titolo pubblicazione Rivista Anno link Scopus link Sci_Dir
A Silica-Supported Catalyst Containing 9-Amino-9-deoxy-9-epi-quinine and a Benzoic Acid Derivative for Stereoselective Batch and Flow Heterogeneous Reactions European Journal of Organic Chemistry 2019 Sci_Dir
CF3: An overlooked chromophore in VCD spectra. A review of recent applications in structural determination RSC Advances 2019 Sci_Dir
Determination of the absolute configuration of conformationally flexible molecules by simulation of chiro-optical spectra: A case study RSC Advances 2019 Sci_Dir
Four-Fold Alkyne Benzannulation: Synthesis, Properties, and Structure of Pyreno[ a]pyrene-Based Helicene Hybrids Organic Letters 2019 Sci_Dir
Insights into the Phytochemistry of the Cuban Endemic Medicinal Plant Phyllanthus orbicularis: Fideloside, a Novel Bioactive 8-C-glycosyl 2,3-Dihydroflavonol Molecules 2019 Sci_Dir
Synthesis of Heterohelicenes by a Catalytic Multi-Component Povarov Reaction European Journal of Organic Chemistry 2019 Sci_Dir
Anno: 2018
Titolo pubblicazione Rivista Anno link Scopus link Sci_Dir
Direct analysis of chiral active pharmaceutical ingredients and their counterions by ultra high performance liquid chromatography with macrocyclic glycopeptide-based chiral stationary phases Journal of Chromatography A 2018 Sci_Dir
Enantioselective ultra high performance liquid and supercritical fluid chromatography: The race to the shortest chromatogram Journal of Separation Science 2018 Sci_Dir
Recent developments in chiral separations by supercritical fluid chromatography Chiral Analysis: Advances in Spectroscopy, Chromatography and Emerging Methods: Second Edition 2018 Sci_Dir
Recognition mechanism of aromatic derivatives resolved by argentation chromatography: The driving role played by substituent groups Analytica Chimica Acta 2018 Sci_Dir
Stereochemical Stability and Absolute Configuration of Atropisomeric Alkylthioporphyrazines by Dynamic NMR and HPLC Studies and Computational Analysis of HPLC-ECD Recorded Spectra European Journal of Organic Chemistry 2018 Sci_Dir
Thioethyl-Porphyrazine/Nanocarbon Hybrids for Photoinduced Electron Transfer Advanced Functional Materials 2018 Sci_Dir
Unmatched Kinetic Performance in Enantioselective Supercritical Fluid Chromatography by Combining Latest Generation Whelk-O1 Chiral Stationary Phases with a Low-Dispersion in-House Modified Equipment Analytical Chemistry 2018 Sci_Dir
Anno: 2017
Titolo pubblicazione Rivista Anno link Scopus link Sci_Dir
Cannabis through the looking glass: Chemo- and enantio-selective separation of phytocannabinoids by enantioselective ultra high performance supercritical fluid chromatography Chemical Communications 2017 Sci_Dir
Capillary methacrylate-based monoliths by grafting from/to γ-ray polymerization on a tentacle-type reactive surface for the liquid chromatographic separations of small molecules and intact proteins Journal of Chromatography A 2017 Sci_Dir
Chiral Peropyrene: Synthesis, Structure, and Properties Journal of the American Chemical Society 2017 Sci_Dir
Chiral Peropyrene: Synthesis; Structure; and Properties Journal of the American Chemical Society 2017 Sci_Dir
Chiral Separations. Chiral Dynamic Chromatography in the Study of Stereolabile Compounds Handbook of Advanced Chromatography/ Mass Spectrometry Techniques 2017 Sci_Dir
Equilibrium condition and stabilization kinetics of lactic acid oligomers in aqueous solutions Canadian Journal of Chemical Engineering 2017 Sci_Dir
Future perspectives in high efficient and ultrafast chiral liquid chromatography through zwitterionic teicoplanin-based 2-μm superficially porous particles Journal of Chromatography A 2017 Sci_Dir
“Click” hyaluronan based nanohydrogels as multifunctionalizable carriers for hydrophobic drugs Carbohydrate Polymers 2017 Sci_Dir
Anno: 2016
Titolo pubblicazione Rivista Anno link Scopus link Sci_Dir
Atropisomerism in 3-arylthiazolidine-2-thiones. A combined dynamic NMR and dynamic HPLC study Organic and Biomolecular Chemistry 2016 Sci_Dir
Chiroptical properties of the ground and excited states of two thia-bridged triarylamine heterohelicenes Journal of Photochemistry and Photobiology A: Chemistry 2016 Sci_Dir
Dynamic Behavior of Clobazam on High-Performance Liquid Chromatography Chiral Stationary Phases Chirality 2016 Sci_Dir
Experimental evidence of the kinetic performance achievable with columns packed with new 1.9 μm fully porous particles of narrow particle size distribution Journal of Chromatography A 2016 Sci_Dir
High-Performance Liquid Chromatographic Resolution of Neutral and Cationic Hetero[6]Helicenes Chirality 2016 Sci_Dir
Pirkle-type chiral stationary phase on core–shell and fully porous particles: Are superficially porous particles always the better choice toward ultrafast high-performance enantioseparations? Journal of Chromatography A 2016 Sci_Dir
Rationale behind the optimum efficiency of columns packed with new 1.9 μm fully porous particles of narrow particle size distribution Journal of Chromatography A 2016 Sci_Dir
Ultra-fast high-efficiency enantioseparations by means of a teicoplanin-based chiral stationary phase made on sub-2μm totally porous silica particles of narrow size distribution Journal of Chromatography A 2016 Sci_Dir
Anno: 2015
Titolo pubblicazione Rivista Anno link Scopus link Sci_Dir
Diastereomer Interconversion via Enolization: A Case Study Chirality 2015 Sci_Dir
Expanding the potential of chiral chromatography for high-throughput screening of large compound libraries by means of sub-2μm Whelk-O 1 stationary phase in supercritical fluid conditions Journal of Chromatography A 2015 Sci_Dir
Highly versatile nanohydrogel platform based on riboflavin-polysaccharide derivatives useful in the development of intrinsically fluorescent and cytocompatible drug carriers Carbohydrate Polymers 2015 Sci_Dir
Polyaspartamide-Doxorubicin Conjugate as Potential Prodrug for Anticancer Therapy Pharmaceutical Research 2015 Sci_Dir
Vibrational Circular Dichroism (VCD) Reveals Subtle Conformational Aspects and Intermolecular Interactions in the Carnitine Family Chirality 2015 Sci_Dir
Anno: 2014
Titolo pubblicazione Rivista Anno link Scopus link Sci_Dir
Dynamic high performance liquid chromatography on chiral stationary phases. Low temperature separation of the interconverting enantiomers of diazepam; flunitrazepam; prazepam and tetrazepam Journal of Chromatography A 2014 Sci_Dir
Enantioseparation by ultra-high-performance liquid chromatography TrAC - Trends in Analytical Chemistry 2014 Sci_Dir
Helical sense-responsive and substituent-sensitive features in vibrational and electronic circular dichroism; in circularly polarized luminescence; and in raman spectra of some simple optically active hexahelicenes Journal of Physical Chemistry C 2014 Sci_Dir
Isolation and identification of 2;4;6-trihydroxyphenanthrene as a byproduct of trans-resveratrol photochemical isomerization and electrocyclization Journal of Organic Chemistry 2014 Sci_Dir
Revealing the fine details of functionalized silica surfaces by solid-state NMR and adsorption isotherm measurements: The case of fluorinated stationary phases for liquid chromatography Chemistry - A European Journal 2014 Sci_Dir
Separation of complex sugar mixtures on a hydrolytically stable bidentate urea-type stationary phase for hydrophilic interaction near ultra high performance liquid chromatography Journal of Separation Science 2014 Sci_Dir
The evolution of chiral stationary phases from HPLC to UHPLC LC-GC Europe 2014
Thermodynamic and kinetic investigation of monoketo-aldehyde- peroxyhemiacetal (MKA); a stereolabile degradation product of dihydroartemisinin RSC Advances 2014 Sci_Dir
Toward enantioselective nano ultrahigh-performance liquid chromatography with Whelk-O1 chiral stationary phase Electrophoresis 2014 Sci_Dir
Yonemitsu-type condensations catalysed by proline and Eu(OTf)3 RSC Advances 2014 Sci_Dir
Anno: 2013
Titolo pubblicazione Rivista Anno link Scopus link Sci_Dir
Analysis of bovine milk caseins on organic monolithic columns: An integrated capillary liquid chromatography-high resolution mass spectrometry approach for the study of time-dependent casein degradation Journal of Chromatography A 2013 Sci_Dir
Bidentate urea-based chiral selectors for enantioselective high performance liquid chromatography: Synthesis and evaluation of "Crab-like" stationary phases Journal of Chromatography A 2013 Sci_Dir
Chiral Supramolecular selectors for Enantiomer differentiation in liquid chromatography Topics in Current Chemistry 2013 Sci_Dir
Raman and ROA spectra of (-)- and (+)-2-Br-Hexahelicene: Experimental and DFT studies of a π-conjugated chiral system Journal of Physical Chemistry B 2013 Sci_Dir
Thermal behaviour of poly(dimethylsiloxane) hybrid silicas prepared by radiation grafting Journal of Thermal Analysis and Calorimetry 2013 Sci_Dir
Anno: 2012
Titolo pubblicazione Rivista Anno link Scopus link Sci_Dir
Design and evaluation of hydrolytically stable bidentate urea-type stationary phases for hydrophilic interaction chromatography Journal of Chromatography A 2012 Sci_Dir
Enantioselective supramolecular carriers for nucleoside drugs. A thermodynamic and kinetic gas phase investigation Journal of the American Society for Mass Spectrometry 2012 Sci_Dir
Enantioselective ultra-high and high performance liquid chromatography: A comparative study of columns based on the Whelk-O1 selector Journal of Chromatography A 2012 Sci_Dir
Inductive and Mesomeric Effects of the [60]Fulleropyrrolidine Fragment and [60]Fullerene Sphere: A Quantitative Evaluation Based on Theory and Experiments European Journal of Organic Chemistry 2012 Sci_Dir
Introducing enantioselective ultrahigh-pressure liquid chromatography (eUHPLC): Theoretical inspections and ultrafast separations on a new sub-2-μm Whelk-O1 stationary phase Analytical Chemistry 2012 Sci_Dir
The dynamic chromatographic behavior of tri-o-thymotide on HPLC chiral stationary phases Chemical Communications 2012 Sci_Dir
Anno: 2011
Titolo pubblicazione Rivista Anno link Scopus link Sci_Dir
Application of circular dichroism spectroscopy in the study of mixed-valence asymmetric ruthenium polypyridyl complexes Inorganic Chemistry 2011 Sci_Dir
Efficient organic monoliths prepared by γ-radiation induced polymerization in the evaluation of histone deacetylase inhibitors by capillary(nano)-high performance liquid chromatography and ion trap mass spectrometry Journal of Chromatography A 2011 Sci_Dir
Immobilized trypsin on epoxy organic monoliths with modulated hydrophilicity: Novel bioreactors useful for protein analysis by liquid chromatography coupled to tandem mass spectrometry Journal of Chromatography A 2011 Sci_Dir
NMR and computational investigations of the chiral discrimination processes involving a cyclic tetraamidic chiral selector European Journal of Organic Chemistry 2011 Sci_Dir
Stereolability of dihydroartemisinin; an antimalarial drug: A comprehensive kinetic investigation. Part 2 Journal of Organic Chemistry 2011 Sci_Dir
Stereolability of dihydroartemisinin; an antimalarial drug: A comprehensive thermodynamic investigation. Part 1 Journal of Organic Chemistry 2011 Sci_Dir
Anno: 2010
Titolo pubblicazione Rivista Anno link Scopus link Sci_Dir
Chiral recognition in aggregates formed by chiral bola-amphiphiles Tetrahedron Asymmetry 2010 Sci_Dir
Extending the use of "Inverted Chirality Columns Approach" for enantiomeric excess determination in absence of reference samples: Application to a water-soluble camptothecin derivative Journal of Chromatography A 2010 Sci_Dir
Hybrid polyacrylamide chiral stationary phases for HPLC prepared by surface- initiated photopolymerization Journal of Separation Science 2010 Sci_Dir
Stereodynamic investigation of labile stereogenic centres in dihydroartemisinin Molecules 2010 Sci_Dir
Anno: 1994
Titolo pubblicazione Rivista Anno link Scopus link Sci_Dir
Stereoselective Heteroaromatic Homolytic Substitution with Carbon Radicals Derived from Oppolzer's Camphorsultam Synlett 1994 Sci_Dir

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